Abstract

It was shown that the remarkable discrepancy among reported proton nuclear magnetic resonance (1H NMR) spectra of 3-deazaadenosine obtained under comparable conditions is actually a reflection of a difference in molecular species, one being neutral and another being cationic, by carefully measuring the 1H NMR spectra of 3-deazaadenosine and its hydrochloride as well as 3-deazaadenine derivatives, whose preparation is also described.

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