Abstract
The crystal structure of η 5-C 5H 5(CO) 3MoHgCl has been determined from single crystal X-ray data collected by counter methods. The compound crystallizes in space group P42 1c with 8 molecules per unit cell and lattice constants of a 12.014(4), c 15.322(7). Full-matrix least squares refinement gave discrepancy factors R 1 0.058 and R 2 0.062 for 854 data with 1 3σ (1). The critical bond lengths and angles are MoHg 2.673(3)Å, HgCl 2.437(8)Å, and MoHgCl 160.0(2)°. Crystals of η 5C 5H 5(CO) 3WHgBr were shown to be isomorphous with lattice constants of a 12.068(4)Å and c 15.643(7)Å.
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