Abstract
Chapter 1 - Introduction and motivation Chapter 2 - Structure and cobalt oxidation state Chapter 3 - Role of anions and redox-inert cations for structure and function Chapter 4 - Cobalt L-edge and oxygen K-edge spectroscopy for complementary insights into the electronic structure of the CoCat Chapter 5 – Shared structural motifs in cobalt-based and nickel-based catalysts Chapter 6 - Investigation of catalyst wear by in-situ XAS Chapter 7 - Changes of oxidation state and structure with the electrode potential Chapter 8 - In-situ XAS experiments on the interrelation of pH and electric potential Chapter 9 - Mode of catalysis in the amorphous CoCat Chapter 10 - Key results Appendix A - Additional experimental detail Appendix B – Analytic solution of the modified Nernst equation
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