Abstract
The structure of monoclinic V 3S 4 was refined using single crystal X-ray data. This modification crystallizes isostructural with Cr 3S 4, space group C2/ m with a = 1263.8(2) pm, b = 329.4(1) pm, c = 587.8(1) pm and β = 115.68(1)°. The sulfur-metal distances are quite similar to those reported for the hexagonal modification of V 3S 4. Nevertheless, the monoclinic modification leaves smaller empty channels than those observed in the hexagonal modification.
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