Abstract
Tricarbonyl[(5,6-η)-dimethyl 7-(p-chlorophenyl)-7- azabicyclo[2.2.1]hepta-2,5-diene-2,3-dicarboxylate- κN]iron(0), [Fe(C 16 H 14 ClNO 4 )(CO) 3 ], was synthesized and structurally characterized. The Fe-CO distances are 1.801 (3), 1.800 (3) and 1.141 (3) A. The Fe-N distance is 2.064 (2) A. The Fe atom interacts with the unsubstituted olefinic bond. The two Fe-C distances are 2.030 (3) and 2.028 (2) A. The C-C distances for substituted and unsubstituted double bonds are 1.341 (3) and 1.424 (3) A, respectively. Two H atoms attached to the coordinated double bond are 0.36 (4) A away from the least-squares plane of C1C2C3C4
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