Abstract
C 25 H 30 BBrO 6 , M r =517.23, monoclinic, P2 1 , a=9.1584 (14), b=6.910 (3), c=20.224 (4) A, β=96.241 (14) o , V=1272.3 (6) A 3 , Z=2, D x =1.350 g cm -3 , λ(Mo Kα)=0.71069 A, μ=16.3 cm -1 , F(000)=535.62, T=230 (1) K, final R=0.041 for 1531 observed reflections. A reactive intermediate in the dialkylboron bromide promoted opening of tartrate acetals by higher-order cuprates has been isolated and characterized by X-ray crystallography
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