Abstract
[Fe(C 7 H 5 N) 4 (C 25 H 21 P 2 )]ClO 4 •0,37C 5 H 5 N cristallise dans P2 1 /n avec a=13,912, b=21,518, c=18,705 A, β=107,86°, Z=4; affinement jusqu'a R=0,083. La structure est composee d'un cation complexe et d'un anion desordonne perchlorate, solvatee par une molecule de pyridine, qui est tres desordonnee. Son meilleur facteur d'occupation converge vers 0,37. Le cation presente une coordination octaedrique deformee autour de l'atome de fer
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More From: Acta Crystallographica Section C Crystal Structure Communications
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