Abstract
Cu(I)catalyzed 1,4-Grignard reaction of the key compound 6 led to the bicyclic keto ethers 7 - 15 together with small amounts of the alcohols 16 - 25 . Wolff-Kishner reduction of 8 - 15 gave the 1,8-cineol homologues 26 - 32 and sesquicineol ( 2 ). - The fresh and camphoraceous odor of 1 changes stepwise with increasing side chain to herbaceous and spicy notes, compounds with branched side chains show lavender undertones. 2 has a pleasant fruity, floral and sweet fragrance.
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