Abstract
The crystal structure of [FeCp((-)diop)I] has been determined by x-ray analysis and refined by least squares methods to R = 0.091 for 1603 independent reflections. The complex crystallises in the orthorhombic space group P2 12 12 1 with a unit cell of dimensions a = 16.920 (3), b = 19.902(4), c = 10.649(6)». The conformation of the chelated (-)DIOP is analysed and compared with those occuridng in other complexes of known structures.
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