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Abstract
The crystal structure of ammonium hydrazinium sulfate, (NH 4) 2N 2H 6(SO 4) 2, is reported for the first time. This compound crystallizes in a unimolecular unit cell in the triclinic space group P 1 with a = 5.600, b = 5.595, c = 8.608 Å, α = 72.47, β = 74.13 and γ = 66.14°. Hydrogen bonding is noted between the sulfate ion and both the ammonium and hydrazinium ions. The room temperature Raman and infrared spectra have been measured. Band assignments of internal and external optic modes are proposed, aided by comparison with spectra of the parent compounds, ammonium sulfate and hydrazinium sulfate. A differential scanning calorimetry measurement indicates phase transitions at 56 and 125°C.
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