Abstract

AZ91D magnesium alloy samples were treated by micro-arc discharge oxidation (MDO) using two different voltage modes: direct current (dc) and high-frequency bipolar pulsing (BP) to improve the surface properties. The structure, composition, and mechanical characteristics of the oxide films prepared using the same average current density were investigated by scanning electron microscopy (SEM), energy-dispersive X-ray spectrometry (EDS), X-ray diffraction (XRD), optical microscopy, profilometry, as well as microhardness and pin-on-disk tests. Both the dc and BP oxide films have mainly the MgO phases and improved microhardness and lower wear rates compared to the untreated Mg alloy. However, the oxidation rate, composition, and structure are different for the two voltage modes. For the same treatment time, the BP mode gives a higher oxidation rate. The BP film is denser and has higher micro-hardness, lower friction coefficient, and smaller weight loss against steel in the scratch test. Our results thus indicate that high-frequency, bipolar pulsing MDO yields a better coating on the Mg alloy.

Talk to us

Join us for a 30 min session where you can share your feedback and ask us any queries you have

Schedule a call

Disclaimer: All third-party content on this website/platform is and will remain the property of their respective owners and is provided on "as is" basis without any warranties, express or implied. Use of third-party content does not indicate any affiliation, sponsorship with or endorsement by them. Any references to third-party content is to identify the corresponding services and shall be considered fair use under The CopyrightLaw.