Abstract
Hyperfine coupling constants of isotopically substituted cyclohexadienyl radicals have been measured as a function of temperature by muon spin rotation and level-crossing spectroscopy. Data are presented for the muon, proton and deuteron hyperfine couplings of the methylene groups in C 6H 6Mu and C 6D 6Mu, and also for all the 13C hyperfine couplings of 13C 6H 6Mu. Comparison of the results with semi-empirical calculations supports a planar ring configuration with complex motion of the methylene substituents.
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