Abstract
Bi-based superconducting phases have been studied by transmission electron microscopy. The strong one-dimensional modulations in undoped and Ce-doped monoclinic Bi2 Sr2 CuO6 (2201) samples are different from one another. We have found a new 2201 phase containing Pb and Ca with orthorhombic symmetry in nominal (Bi0.90 Pb0.10 )2 Sr2 CaCu2 O8 crystals. Its structure with space group Bbmb and two-dimensional modulation are analogous to those of the Pb-doped higher members of the structural series Bi2 Sr2 Can−1 Cun O2n+4 . Hence, this new orthorhombic rather than the monoclinic 2201 phase should be the first member of the structural series.
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