Abstract
Zirconium phosphate-phosphite have various structure belonging to the drying heat of the sample. While sample dried above sat. NaCl solution had interlayer distance of 1.30 nm (result fromd1=0.74 nm andd2=0.56 nm for phosphite layer), the sample dried under IR lamp on air having interlayer spacingd=0.74 nm charactderistic for α-Zr(HPO4)2·H2O containing little amount of phosphite groups. The composition of the first sample can be characterized by chemical formula, as Zr(HPO4)0.7(HPO3)1.3· ·0.5H2O. The X-ray powder diffraction data ofn-butylamine intercalate suggest that in the process take place only the phosphate region of zirconium phosphate-phosphite (ZrPP).
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