Abstract

We have synthesized and characterized the first known 2,2- trans isomer of the N-substituted dirhodium(II) tetrakisacetamidate, Rh 2(RNAc) 4, class of compounds. The bis benzonitrile adduct exhibits a unique orthogonal arrangement of the axial aromatic rings in the solid state. Structural and electronic features suggest the presence of π-backbonding.

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