Stress sensitivity of multiscale elastic properties under hydrostatic loading conditions of organic shales at different thermal maturity stages

Abstract

Shales serve essential functions as seals for conventional hydrocarbon reservoirs, waste storage repositories and unconventional plays. Exploration and evaluation of shales rely on the characterization of their multiscale elastic properties. However, there are limited studies on the geologic controls of elastic stress sensitivity in organic shales. This study investigated dry Lokpanta, Bakken, and Niobrara shales of different thermal maturity stages. First, we used a pulse-transmission ultrasonic setup to conduct multidirectional (0o, 45o and 90o) hydrostatic-stress sensitivity (0–27.58 MPa) tests to measure elastic waves and derive other elastic properties. Furthermore, we inverted microscopic parameters from the elastic measurements based on effective medium theories such as damage parameters (αij and βijkl), crack density (ρ), normal to tangential microcrack compliance (B), specific tangential crack compliance (snBT) and microcracks orientation anisotropy (η). Finally, we studied the effects of organic matter maturity and clay diagenesis on the multi-scaled elastic stress sensitivity. Under applied hydrostatic stress, the non-linear elastic response in the shales is consistent with the closure of aligned microcracks. Microcrack closure decreased the elastic anisotropy at lower stress (<10 MPa), while aligned clays and organic matter control the stress-insensitive anisotropy at higher stress. As organic matter matures and smectite transforms to illite, orthogonal velocity stress sensitivity increases and extrinsic contribution to elastic anisotropy increases. There is also a corresponding increase in orthogonal damage second-rank tensor (α33) and a decrease in orthogonal damage fourth-rank tensor (β3333) with organic matter-clay thermal maturity. These relationships are due to the thermally-induced development of new and/or extensional roughly-textured microcracks parallel to the laminated microfabric, which is of higher compliance in the shear than compression. Microcrack closure also decreases ρ under applied pressure. Most of the samples had B < 0.5, suggesting the presence of non-idealized roughly textured microcracks. Generally, snBT broadly decreases and η increases with clay diagenesis and organic matter maturity also because of the generation and/or enhancement of aligned microcracks resulting in higher tangential stiffness.