Abstract
AbstractA highly stereoselective total synthesis of attenols A and B is described. The salient features of this synthesis are the utilization of a reductive radical cyclization strategy for methyl center creation, a Prins cyclization/reductive opening cascade for anti‐1,3‐diol motif generation, and a double alkylation tosylmethyl isocyanide (TosMIC) strategy to construct the spiro acetal segment.
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