Abstract
Methyl 2,3-dideoxy-DL-pent-2-enopyranosid-4-ulose ( 2) and 1- O-benzoyl-2,3- dideoxy-DL-pent-2-enopyranos-4-ulose ( 3), obtained from furfuryl alcohol, gave methyl β-DL- erythro-pentopyranosid-4-ulose ( 6) and 1- O-benzoyl-β-DL- erythro-pentopyranos-4-ulose ( 7), respectively, on cis-hydroxylation with silver chlorate- osmium tetroxide. Reduction of the isopropylidene derivatives ( 8 and 9) of 6 and 7 with lithium aluminium hydride and sodium borohydride, respectively, afforded DL-ribose derivatives.
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