Abstract
A stereoretentive trifluoromethylthiolation of styrylboronic acids with AgSCF3 or N-trifluoromethylthiosuccinimide has been developed under mild reaction conditions. This synthetic method for vinyl trifluoromethyl thioethers possesses good functional group tolerance, high yield and excellent stereoselectivity with AgSCF3 as the SCF3 source. The stereospecificity of the reaction could been achieved through the trifluoromethylthiolation of β‑styrylboronic acids with N-trifluoromethylthiosuccinimide.
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