Abstract

AbstractTo study the metabolism of minor conjugated linoleic acid isomers (CLAs), (7E,9Z)‐[9,10‐2H] CLA was prepared in three steps from a conjugated enyne precursor. In the labelling step, deuterium atoms were introduced by partial reduction of the triple bond using deuterated disiamylborane and acetic acid‐d4. Deuterated (7E,9Z) CLA was obtained with high isotopic enrichment (>99%) and purity greater than 95%. Copyright © 2004 John Wiley & Sons, Ltd.

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