Abstract
Abstract The stepwise synthesis of AuI4CoIII2 complex with d-penicillaminate and 1,2-bis(dicyclohexylphosphino)ethane, [2]2+, via metalloligand approach, together with single-crystal X-ray analysis of nitrate salt, [2](NO3)2, is reported. [2](NO3)2 adopts normal alternate arrangement of cations and anions in crystal, which is different from non-alternate arrangement in corresponding AuI4CoIII2 complex with d-penicillaminate and 1,2-bis(diphenylphosphino)ethane.
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