Abstract

For the best possible limit of detection of any thin film-based magnetic field sensor, the functional magnetic film properties are an essential parameter. For sensors based on magnetostrictive layers, the chemical composition, morphology and intrinsic stresses of the layer have to be controlled during film deposition to further control magnetic influences such as crystallographic effects, pinning effects and stress anisotropies. For the application in magnetic surface acoustic wave sensors, the magnetostrictive layers are deposited on rotated piezoelectric single crystal substrates. The thermomechanical properties of quartz can lead to undesirable layer stresses and associated magnetic anisotropies if the temperature increases during deposition. With this in mind, we compare amorphous, magnetostrictive FeCoSiB films prepared by RF and DC magnetron sputter deposition. The chemical, structural and magnetic properties determined by elastic recoil detection, X-ray diffraction, and magneto-optical magnetometry and magnetic domain analysis are correlated with the resulting surface acoustic wave sensor properties such as phase noise level and limit of detection. To confirm the material properties, SAW sensors with magnetostrictive layers deposited with RF and DC deposition have been prepared and characterized, showing comparable detection limits below 200 pT/Hz1/2 at 10 Hz. The main benefit of the DC deposition is achieving higher deposition rates while maintaining similar low substrate temperatures.

Highlights

  • Surface acoustic wave (SAW) devices constitute a multifunctional sensor concept [1]

  • A wide range of ferromagnetic materials are used for the magnetic sensitive layer, e.g., FeCo, FeGa, Fe2Tb and (Fe90Co10)78Si12B10 (FeCoSiB) [10,11,12], which are deposited on the SAW sensor as full films, multilayers or patterned structures [12,13,14]

  • The shown research is based on ST-cut quartz SAW devices with a full film FeCoSiB layer based on previous studies [5,8,9] with a focus on the deposition process of the magnetic sensitive layer with regard to material composition, magnetic anisotropy, film stress, amorphicity and overall sensor performance

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Summary

Introduction

Surface acoustic wave (SAW) devices constitute a multifunctional sensor concept [1]. The use of different piezoelectric substrates and crystallographic orientations allows the excitation of various types of surface acoustic waves, like seismic waves such as Rayleigh waves or shear horizontal waves called Love waves. Using opposite output IDTs, the voltage generated in the piezoelectric material by the transmitted and influenced shear wave is recorded and the phase change between input and output signal serves as a measure of the applied magnetic field In this case, a magnetostrictive layer was deposited from a magnetron sputter target with the composition (Fe90Co10)78Si12B10 (FeCoSiB) on top of the delay line. FeCoASfitBer aitrheasnboeteincedaebmloen.strated that both deposition methods DC and RF lead to the same layer composition and structure, the control of film stress and imprinted magnetic anisotropy become important parameters for the following magnetic samples and SAW sensors. SAW Sensor Performance As shown in the previous chapter, a uniaxial anisotropy cannot be induced precisely

SAW Sensor Performance
Conclusions
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