Abstract
Multiple inorganic fullerene-like (IF) molybdenum disulfide hollow spheres were synthesized through spray drying method. The molybdenum trisulfide precursor, which was prepared by the mixed solution of ammonium molybdate ((NH 4) 2MoO 4) and ammonium disulfide ((NH 4) 2S) with a spray drying method, was desulfurized at 850 °C in a mixture of hydrogen and argon, and subsequently multiple fullerene-like molybdenum disulfide hollow spheres were obtained. The samples were identified and characterized by X-ray powder diffraction (XRD), field-emission scanning electron microscopy (SEM), and high-resolution transmission electron microscopy (HRTEM), and the mechanism of formation is also discussed based on the experimental result. The spray drying process would be an effective method to synthesize large-scale of inorganic fullerene-like materials.
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