Abstract
We have found that the line shape in 31P magic-angle spinning (MAS) NMR spectra is dependent on the spinning rate of the sample for pyrophosphates and metaphosphates such as Na 4P 2O 7, Na 4P 2O 7·10H 2O, Ag 4P 2O 7, and (KPO 3) n . The dependence can be explained by spectral spin diffusion of 31P spins through dipole-dipole interaction.
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