Abstract
Knowledge-based catalyst development is always an interaction between preparation, analysis and catalytic testing [...]
Highlights
Since the beginning of the century, operando, or in-situ, spectroscopy has played an increasing role in the analysis of catalysts [1,2]
Whereas in-situ methods work under catalytic conditions, operando combines in-situ spectroscopy with catalytic activity [1], or, in other words, analytics and catalytic testing
Compromises must be made, because the ideal conditions for spectroscopic measurements with good signal/noise ratios do not fit with real catalytic conditions, comprising high pressure, high temperature and sometime aggressive compounds which could destroy the sensitive parts of the spectroscopic equipment
Summary
Since the beginning of the century, operando, or in-situ, spectroscopy has played an increasing role in the analysis of catalysts [1,2]. Knowledge-based catalyst development is always an interaction between preparation, analysis and catalytic testing. Whereas in-situ methods work under catalytic conditions, operando combines in-situ spectroscopy with catalytic activity [1], or, in other words, analytics and catalytic testing.
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