Abstract
A new diiodo-containing compound, fully substituted derivative of benzoic acid was successfully synthesized in quantitative yield using iodine/silver trifluoroacetate as an efficient iodinium donating reagent. The obtained 2,6-diiodo-3,4,5-trimethoxybenzoic acid was analyzed structurally by FT-IR, 1H NMR, and 13C NMR spectroscopic techniques and was additionally compared with optimized structure and harmonic vibrational frequencies predicted by quantum chemical calculations. Peculiar spectral features as a result of intramolecular interactions between neighboring iodo and carboxyl functionalities were in a particular focus in the present study.
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