Abstract
A spectral technique for the analysis of complex gas mixtures by isotope dilution is described. The sensitivity of the hydrogen determination in complex mixtures amounts to 0.1% with a relative statistical error of 10%. In similar cases the sensitivity of the nitrogen determination is 0.5% with a relative statistical error of 7–8%. A technique for determining nitrogen and hydrogen simultaneously in complex gas mixtures with a double-slit diffraction monochromator was developed. The optimum operating conditions were established (electrode-less high-frequency discharge, pressure of 8–12 mm Hg, cooled quartz tube with an inside diameter of 1–2 mm for the discharge).
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