Abstract

Monoclinic Nb2O5 nanorod superstructures were first synthesized by a facile yet effective hydrothermal route using Sn2Nb2O7 nanoparticles as the precursor. These unique Nb2O5 nanorod superstructures assembled by small nanorods facilitate the spatial separation of photogenerated charge carriers, thus leading to improved photocatalytic H2 production activity in methanol aqueous solution under ultraviolet light irradiation, which is about 151 times higher than that of commercial Nb2O5 powders.

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