Abstract
Phenyl migration and oxidative addition were observed in nitromethane containing solutions of trans-[RhCl(CO)(SbPh 3) n ] ( n = 2 or 3) and free SbPh 3. A Rh(III) product resulting from phenyl migration and oxidative addition to Rh(I), trans- mer-[Rh(Cl) 2(Ph)(SbPh 3) 3], was characterised by X-ray crystallography.
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