Abstract

Laser Powder Bed Fusion (LPBF) technology was used to produce samples based on the Ti–6Al–4V alloy for biomedical applications. Solid-state phase transformations induced by thermal treatments were studied by neutron diffraction (ND), X-ray diffraction (XRD), scanning transmission electron microscopy (STEM) and energy-dispersive spectroscopy (EDS). Although, ND analysis is rather uncommon in such studies, this technique allowed evidencing the presence of retained β in α’ martensite of the as-produced (#AP) sample. The retained β was not detectable by XRD analysis, nor by STEM observations. Martensite contains a high number of defects, mainly dislocations, that anneal during the thermal treatment. Element diffusion and partitioning are the main mechanisms in the α ↔ β transformation that causes lattice expansion during heating and determines the final shape and size of phases. The retained β phase plays a key role in the α’ → β transformation kinetics.

Highlights

  • Metal additive manufacturing is taking the lead in market sections where low production volumes, freedom of design, and a high level of customization are the guiding lights, such as in biomedical and aerospace markets [1,2]

  • A Ti–6Al–4V alloy has been produced by Laser Powder Bed Fusion (LPBF), following the material processing used in the production of commercial devices employed in dentistry

  • The aim of the present paper is to investigate phase transitions induced by thermal treatments performed on Ti–6Al–4V samples produced by LPBF

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Summary

Introduction

Metal additive manufacturing is taking the lead in market sections where low production volumes, freedom of design, and a high level of customization are the guiding lights, such as in biomedical and aerospace markets [1,2]. This manufacturing technique is suitable for strategic metallic materials, which are difficult and expensive to manufacture with traditional subtractive technologies. Low-speed machining of forged titanium has been successfully employed over history, resulting in more than half of the raw materials wasted as scrap [5,6].

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