Abstract
ABSTRACT Lead lanthanum zirconate titanate (PLZT) fibers, Pb1 - xLax(Zr1 - yTiy)1 − x/4 O3 were prepared using sol-gel technique with y = 0.35 and x as 0.09. Lead acetate, lanthanum nitrate, zirconium acetate and tetra isopropyl orthotitanate were used as the precursor materials to obtain a sol, which was concentrated to spinnable consistency by polymerizing in a rotary evaporator at 70°C. The gel fibers obtained via spinning method were calcined at 500°, 850° and 1200°C to get the ceramic fibers. Fourier transform infrared (FTIR) spectroscopy, X-ray diffraction, Thermogravimetric analysis (TGA) and scanning electron microscopy (SEM) were used to characterize the fibers. X-ray analysis showed that pure perovskite phases were obtained at 850°C. The microstructure showed the presence of fibers with smooth structure.
Sign-in/Register to access full text options 
Talk to us
Join us for a 30 min session where you can share your feedback and ask us any queries you have
Schedule a callDisclaimer: All third-party content on this website/platform is and will remain the property of their respective owners and is provided on "as is" basis without any warranties, express or implied. Use of third-party content does not indicate any affiliation, sponsorship with or endorsement by them. Any references to third-party content is to identify the corresponding services and shall be considered fair use under The CopyrightLaw.
