Softening and dynamic recrystallization in magnesium single crystals during c-axis compression

Abstract

Commercial purity (99.8%) magnesium single crystals were subjected to plane strain compression (PSC) along the c-axis at 200 and 370 °C and a constant strain rate of 10 −3 s −1. Extension was confined to the 〈 1 1 2 ¯ 0 〉 direction and the specimens were strained up to a logarithmic true strain of −1. The initial rapid increase in flow stress was followed by significant work softening at different stresses and comparable strains of about −0.05 related to macroscopic twinning events. The microstructure of the specimen after PSC at 200 °C was characterized by a high density of { 1 0 1 ¯ 1 } and { 1 0 1 ¯ 3 } compression twins, some of which were recrystallized. After PSC at 370 °C, completely recrystallized twin bands were the major feature of the observed microstructure. All new grains in these bands retained the same c-axis orientation of their compression twin hosts. The basal plane in these grains was randomly rotated around the c-axis, forming a fiber texture component. The obtained results are discussed with respect to the mechanism of recrystallization, the specific character of the boundaries between new grains and the initial matrix, and the importance of the dynamically recrystallized bands for strain accommodation in these deformed magnesium single crystals.