Abstract
The sulfinatodeiodination reagent Ce4+ −NaHSO3 was shown to be able to initiate the addition of perfluoroalkyl iodides to olefins at 50—70°C to give the corresponding adducts in good yield. Similarly, SO2− generated from Fe3+−NaHSO3 system can also initiate the same addition although the reagent is not able to cause sulfinatodeiodination. Furthermore it was shown that sodium perfluoroalkanesulfinate is able to initiate the same addition and there is no exchange between the perfluoroalkyl groups of R'FSO2Na and RFI.
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