Abstract
[63640-54-0] C10H12ClNO3S (MW 261.75) InChI = 1S/C10H12ClNO3S/c1-16(14,15)12-9(10(11)13)7-8-5-3-2-4-6-8/h2-6,9,12H,7H2,1H3/t9-/m0/s1 InChIKey = AKXYQEYWBQEDKN-VIFPVBQESA-N (chiral reagent for the resolution of racemic alcohols via separation of the corresponding diastereomeric esters1) Physical Data: mp 84–85 °C; [α]D20 +4.3° (c 1.6, THF). Solubility: readily sol THF, benzene, ether. Form Supplied in: pale yellow needles; not available commercially. Preparative Method: prepared from (S)-phenylalanine by reaction with Methanesulfonyl Chloride, followed by Phosphorus(V) Chloride.1b Purification: the crude compound can be recrystallized from hexane/ether. Handling, Storage, and Precautions: best if prepared immediately prior to use. Can be stored at 0 °C under nitrogen for several days without appreciable decomposition.
Sign-in/Register to access full text options 
Free) 
Talk to us
Join us for a 30 min session where you can share your feedback and ask us any queries you have
Schedule a call
