Abstract
The photochemical decarbonylation and rearrangement of the small phosphorus-bridged, σ-metalated pentaborane(9) cluster [Fe(η 5 -C 5 H 5 )(CO) 2 B 5 H 7 (μ-P(C 6 H 5 ) 2 )] (3) was found to produce the organometallic tetraborane cluster complex [Fe(η 5 -C 5 H 5 )(CO)B 4 H 6 (P(C 6 H 5 ) 2 )] (4)
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