Abstract
Specific features and regularities of size distributions of crystalline nuclei are studied using the electrocrystallization of copper and silver on glassy carbon as an example. For a potentiostatic nucleation mode, with increasing overvoltage, a nonuniform size distribution approaches a uniform one. For a galvanostatic nucleation mode, the most probable nuclei size decreases with increasing current density and decreasing concentration of copper ions in solution, and the nuclei size distribution becomes more nonuniform due to a more pronounced non-steady-state nature of galvanostatic nucleation.
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