Abstract
PMMA is often considered as a calibration material for experimental benches dedicated to viscoelasticity investigation. Nevertheless, regarding literature, data concerning attenuation coefficients and quality factors are essentially available in the MHz frequency range and results in the low-frequency range are scarce and scattered. In this communication, thanks to the use of high-frequency ultrasonic spectroscopy between 2 and 8 MHz in the range 6 °C − 45 °C, Time-Temperature Superposition principle and Resonant Ultrasonic Spectroscopy (RUS), we show that both longitudinal and shear quality factors of PMMA decrease considerably for low frequencies (<MHz), and that the classically accepted linear laws describing attenuation as a function of frequency are valid only beyond several MHz. This variation is attributed to secondary relaxation processes such as γ relaxation considering the activation energy deduced from experimental data. Power laws are proposed to describe the evolution of quality factors and attenuation coefficients versus frequency in the 20 kHz − 12 MHz range.
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