Abstract
Nearly all the isomeric hydroperoxides from the reaction of oleic, linoleic and linolenic acids with singlet oxygen are separated in a single analysis by micellar electrokinetic chromatography with polyoxyethylene lauryl ether (Brij 35) as surfactant. Fatty acids tend to adsorb strongly onto the silica, so that coating of the capillary is essential. Brij 35 is used for dynamic coating of either octadecylsilane-derivatised or fused-silica capillaries. A diode array is used for the detection.
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