Abstract
All eight inositols were resolved by liquid chromatography under pressure using a Ca 2+-form cation-exchange resin as stationary phase and water as an eluting solvent. The method was successfully applied to the separation of the products formed when myo-inositol was boiled in water in the presence of Raney nickel. In this case, six peaks corresponding to inositols and at least seven unknown peaks were resolved, showing that this liquid chromatographic method is an efficient way to monitor the side reactions which occur during the 1H 2H exchange reaction of myo-inositol in deuterium oxide with Raney nickel catalyst.
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