Abstract

The analysis of sebum alcoholic mixtures directly by the gas chromatograph is beset by several difficulties such as the overlapping of some of the branched chain peaks, among others. As inherent with most mixtures of biological origin, the resolution or preparation of samples becomes a problem of prime importance. Accordingly, the alcohols obtained on saponification of hair lipids followed by chromatography of the unsaponifiable portion over alumina have been submitted to thin-layer chromatography (TLC) and each of the resulting fractions analyzed by temperature programmed gas chromatography. In this way, a variety of component peaks was afforded for further structural elucidation. Previously, a direct analysis of the alcohol and sterol mixture from hair lipids by gas chromatography without recourse to TLC was advanced by this laboratory (1).

Full Text
Paper version not known

Talk to us

Join us for a 30 min session where you can share your feedback and ask us any queries you have

Schedule a call

Disclaimer: All third-party content on this website/platform is and will remain the property of their respective owners and is provided on "as is" basis without any warranties, express or implied. Use of third-party content does not indicate any affiliation, sponsorship with or endorsement by them. Any references to third-party content is to identify the corresponding services and shall be considered fair use under The CopyrightLaw.