Abstract
The hybrid water electrolysis affords a green route for the generation of fine chemicals accompanied with hydrogen production relying on the rapid development of anodic electrocatalysts. Herein, a nickel‐cobalt layered double hydroxide (NiCo LDH) modified nickel foam, prepared at room temperature via simple soaking processes, could effectively catalyze the dehydrogenation oxidation of primary amines to generate aromatic and aliphatic nitriles with good yields. Further expanding the application of the easily available electrode, the NiCo LDH electrode could function as the electron reservoir to realize the decoupled water electrolysis with 100% coulombic efficiency in the membrane-free electrolytic cell.
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