Abstract
1 atm CO, 30°C, and 10 mol% selenium—these are the conditions under which the S-alkyl thiocarbamates 1 were obtained in 41–100% yield according to Equation (a). The presumed intermediates are selenocarbamates, carbonyl selenide, and carbonyl sulfide. R1,R2 = Et, nPr, nPr, nBu, Ph, H; R3 = Me, Et, PhCH2, 4-ClC6H4CH2.
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