Abstract
A novel method for the synthesis of a N-ethyl-N-(o-tolyl)formamide was described which involves ozonolysis of a cis-crotamiton. The reaction proceeds via ozone attack on the enolic double bond, cleavage, and aldehyde formation through the free hydroxyl group. The present study establishes the conditions for selective ozonolysis of cis-crotamiton, leading to N-ethyl-N-(o-tolyl)formamide 2 (55.7%). The N-ethyl-N-(o-tolyl)formamide was characterized by spectroscopical techniques.
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