Abstract
A novel approach to synthesizing iron trifluoride-filled carbon nanotubes by in situ selectively fluorinating an iron iodide precursor is presented. The potential of this method is explored, demonstrating the successful incorporation of iron trifluoride into the carbon nanotube structure. Various characterization techniques such as X-ray diffraction (XRD), PDF analysis managed at synchrotron, Raman spectroscopy, solid-state NMR, elemental analysis (EDS), and high-resolution transmission electron microscopy (HRTEM) were used to investigate the obtained hybrid nanomaterials. These characterization techniques provided a comprehensive understanding of the FeF3@CNT hybrid nanomaterial, allowing for a thorough analysis of its structural and morphological properties. This knowledge is crucial for further optimizing the material's performance and tailoring it for specific applications in fields such as energy storage, catalysis, or medical uses.
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