Abstract

A method is proposed for selective complexometrie determination of mercury, thiocyanate being used as masking agent. An excess of EDTA is added and the surplus is back-titrated at pH 5–6 with lead nitrate, Xylenol Orange or Methylthymol Blue being used as indicator. Thiocyanate is then added to decompose the mercury-EDTA complex and the liberated EDTA is titrated with lead nitrate. The interference of various cations has been studied.

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