Scanning electron microscopy analysis of non-metallic inclusions for making steels with superior mechanical properties

Abstract

The objective of this novel research was to further understand the type, size and areal distribution of the non-metallic inclusions in bearing steels by applying state-of-the-art scanning electron microscopy (SEM) analysis in order to develop steels with superior properties. Ten samples were taken from bearing steel grade 52100 and analysed by SEM. It was concluded that SEM allows deeper understanding regarding the type, morphology, size, and distribution of the non-metallic inclusions by covering larger sample areas and accurate automatic energy dispersive X-ray microanalysis of the inclusions. While most of the non-metallic inclusions had an equivalent circle diameter (ECD) smaller than 20 µm, the main type of inclusions with ECDs larger than 20 µm were calcium aluminates. As the higher sulphur will tend to create sulphide type of inclusions and the lower sulphur will shift the inclusions towards calcium aluminate oxide types, it is recommended to keep the sulphur content at amounts above threshold that calcium aluminates appear.