Abstract
ST 0 type nuclear spin polarization has been observed in the reaction products of photochemically generated acylalkyl biradicals in the presence of a scavenger. From the magnetic field dependence of biradical CIDNP the rate constant k of proton abstraction from 2-methyl-2-propanethiol by the alkyl site of the biradicals has been determined ( k = 5.0 × 10 7 M −1 s −1).
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