Abstract
A novel C-H acyloxylation method of 1-(1-naphthalen-1-yl)isoquinoline derivatives with peresters in the presence of [Ru(p-cymene)Cl2]2 has been developed. The combination of ruthenium(II), AgBF4, CoI2, and 2,2,6,6-tetramethyl-1-piperidinyloxy is found to be an effective catalytic system to provide various biaryl compounds in satisfactory yields within minutes. Notably, steric hindrance is a very important determinant of the reaction.
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