Abstract
Lignin was extracted from Alamo switchgrass (Panicum virgatum) and yellow polar (Liriodendron tulipifera) by organosolv fractionation at different pretreatment temperatures, and its chemical structure was studied by means of elemental analysis and spectroscopy. Thermal properties of lignins were investigated using thermogravimetric analysis and differential scanning calorimetry. Lignin fibers were produced via melt-spinning by a twin-screw extruder with a custom spinneret. Fibers were thermostabilized at different rates and finally carbonized. In both species, lignin obtained from higher severity organosolv fractionation had fewer impurities, higher content of phenolic hydroxyl groups, and more condensed structures as a result of extensive cleavage of aryl ether linkages. Higher organosolv severity improved the ability to spin fibers; in the case of switchgrass, only the high severity sample was spinnable. High severity also decreased thermostabilization time and increased tensile strength and modulus of ...
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