Abstract

In this research article, we report the role of coupling divalent metal ion tin (Sn) on the structural and magnetic properties of NiFe2O4 nanoparticles (NPs). A series of nanocrystalline nickel ferrites [Ni( $1-x$ )Sn( $x$ )Fe2O4] with composition $x = 0.0$ , 0.2, 0.4, 0.6, and 0.8 are synthesized by coprecipitation method. The synthesized title product is subjected to a variety of analytical techniques such as powder X-ray diffractometer (PXRD), scanning electron microscopy (SEM), and vibrating sample magnetometer (VSM), to understand the structural and magnetic properties. PXRD patterns confirm the single-phase formation of NiFe2O4 NPs as well as Sn concentration. SEM images showed the surface morphology details and size of the particles. VSM studies reveal that the saturation magnetization ( $M_{\mathrm {s}}$ ) of soft superparamagnetic nature reduces with the variation of Sn concentration.

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